This ensures the most durableand reliable performance that has been proven over billionsof cycles through decades of maintenance-free use inElectroForce fatigue test instruments. Range-150 C - 500 C : Sensor Output: Modulus Loss Factor (tan delta) Frequency Range: 0.001 to 1000 Hz : Tan Delta Range: Displacement Range () 1.6 mm : Temperature Range-150 C . High-speed closed-loop controller capable of harnessing even the most dynamic ElectroForce motors, TuneIQ auto-tuning process for simple controller setup, Adaptive amplitude and phase controllers for high-precision control over long-term tests, Controller stability checks provide peace of mind. These two rubber samples have different amounts of filler content, specifically 40 phr and 60 phr, where phr is a batch unit standing for parts per hundred of rubber. These two packages provide advanced algorithms, sophisticated data visualization, and powerful analysis tools for fast and flexible execution and presentation of experiments. TA Instruments. The FCO is the premier temperature device for materials testing and is designed to optimize temperature response time, uniformityand stability. The frequency and magnitude of the deformation can be held constant or varied (swept) during an experiment. The bottom figure shows the results of a fatigue study on thermoplastic elastomers. Available in two models, the ACS-2 and ACS-3, the chillers feature a multi-stage cascading compressor design that is capable of utilizing compressed air (7 bar, 200 l/min) as the cooling medium. They also add highly durable and fast fatigue test methods, delivering as much as 15,000 Newtons of force in the largest HF-DMA model. 3-Point Bending, Dual/Single Cantilever, FilmTension, Compression, 3-Point Bending:5, 10, 15 mm (Fixed-Length), Up to 15 mm (Width), and Up to 7 mm (Thickness)Dual/Single Cantilever:35/17.5 mm (Fixed-Length), Up to 15 mm (Width), and Up to 5 mm (Thickness)Film Tension:5 to 30 mm (Length), Up to 8 mm (Width), and Up to 2 mm (Thickness)Compression:Up to 15 and 40 mm (Diameter), Up to 10 mm (Thickness), TA Instruments109 Lukens Dr.New Castle, DE 19720Phone: 302-427-4000Fax: 302-427-4041Email:answerman@tainst.comWebsite:http://www.tainstruments.comApplication Hotline: 302-427-4070, Irvine Materials Research Institute - Driving Materials Innovation, Laboratory for Electron and X-ray Instrumentation, Center for Transmission Electron Microscopy, Scanning Electron Microscopy & Focused Ion Beam, Low-Mass and High-Stiffness Sample Clamps, Viscoelastic Properties (E, E, and tan ). It is the only motor in theindustry backed by a ten-year warranty. Fatigue and ramp-to-failure tests are easily programmed with a variety of available waveforms including sine, triangle, square, or ramp. TA Instruments invites you to experience the ultimate in Dynamic Mechanical Analyzers, the Discovery DMA 850. endobj Thermal Conductivity & Diffusivity Analyzers, High Pressure Thermogravimetric Analyzers (HP-TGA), Discovery Hybrid Rheometer (DHR) Accessories, Nano Differential Scanning Calorimeter (DSC), ElectroForce Mechanical Testing Accessories, Thermal Conductivity & Diffusivity Brochures, ElectroForce Mechanical Testing Brochures, High Force DMA & Fatigue Test Instruments, 8/4* mm (L), Up to 15 mm (W) and 5 mm (T), 20/10* mm (L), Up to 15 mm (W) and 5 mm (T), 35/17.5* mm (L), Up to 15 mm (W) and 5 mm (T), 5,10, or 15 mm (L), Up to 15 mm (W) and 7 mm (T), 5 to 30 mm (L), Up to 8 mm (W) and 2 mm (T), 5 to 30 mm (L), 5 denier (0.57 tex) to 0.8 mm diameter, Fixed at 15 mm (L), Up to 8 mm (W) and 2 mm (T), 5, 10, or 15 mm (L), Up to 15 mm (W) and 7 mm (T). A unique low-friction, roller bearing supported design available on the 20 mm and 50 mm clamps improves modulus accuracy and reproducibility by accommodating and accounting for twist or curvature in the test specimen. May 1, 2023 - TA Instruments The schematic diagrams of the components of DMA 2980 and a "traditional" DMA are shown in the Figures 1 and 2, respectively. Thermal Conductivity & Diffusivity Analyzers, Melt Viscosity Measurements at High Temperatures, High Temperature Rotational Viscometry of Mold Powder for Continuous Casting, ISO 4664 Rubber, vulcanized or thermoplastic Determination of dynamic properties, ISO 4666 Rubber, vulcanized Determination of temperature rise and resistance to fatigue in flexometer testing, ISO 6721 Plastics Determination of dynamic mechanical properties, ASTM D623 Plastics DMA: Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures, ASTM D4065 Plastics DMA: Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures, ASTM D4473 Standard Test Method for Plastics: Dynamic Mechanical Properties: Cure Behavior, ASTM D5023 DMA testing: Standard Test Method for Measuring the Dynamic Mechanical Properties: In Flexure (Three-Point Bending), ASTM D5024 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Compression, ASTM D5026 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Tension, ASTM D5418 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Flexure (Dual Cantilever Beam), ASTM D5992 Rubber testing: Standard Guide for Dynamic Testing of Vulcanized Rubber and Rubber-Like Materials Using Vibratory Methods, ASTM D7028 Standard Test Method for Glass Transition Temperature (DMA Tg) of Polymer Matrix Composites by Dynamic Mechanical Analysis (DMA), ASTM E1640 DMA testing: Standard Test Method for Assignment of the Glass Transition Temperature By Dynamic Mechanical Analysis, DIN 53513 Determination of the viscoelastic properties of elastomers on exposure to forced vibration at non-resonant frequencies, DIN 53533 Testing of elastomers; testing of heat generation and service life during the fatigue test. 6 0 obj TA Instruments DMA Q800 Dynamic Mechanical Thermal Analysis (DMTA) View DMA BrochureDMA AccessoriesRequest a Quote. TA Instruments. Discover powerful TRIOS software that delivers exceptional user experience in a combined package for instrument control, data analysis and reporting for thermal analysis and rheology. By continuing without changing your cookie settings, you agree to this collection. Data from RPA, MDR, Mooney Viscometer, Hardness, and Density tests can be organized, compared, and analyzed by material type, inventory order, date, and more. Els Verdonck is a Senior Applications Scientist with TA Instruments. She received her degree in Chemical Engineering and her PhD from Brussels . DMA is commonly used to measure glass transition temperatures (Tg) and secondary transitions, orientation caused by processing, cold crystallization, cure optimization, filler effects in composites, and much more. Building on superior technologies of the world's best-selling DMA, improvements in every aspect of DMA performance deliver the most accurate and reproducible measurement of mechanical properties over a wide temperature range. TA Instruments Single user interface with all necessary inputs/outputs to configure test protocols, define acquisition settings, adjust test parameters while a test is running, and real-time monitoring of test progress. High Resolution OpticalDisplacement Sensor. Select Save to download the file to your computer for installation at a later time. <> Enhanced Tzero heat flow technology for the X3 guarantees temperature and enthalpy accuracy simultaneously on all three samples, High-end performance with three sample calorimeters provide unmatched flexibility from replicate testing for statistical analysis to validation/verification against a control sample for the ultimate in certainty. Accurate sample temperature is obtained by a thermocouple placed within the fluid reservoir and close to the sample, Inert stainless steel construction and a seal-free design ensure compatibility with a wide range of fluids, Temperature control provided by the Standard Furnace without additional circulators or environmental systems. TA Instruments Menu Products Products Thermal Analyzers Differential Scanning Calorimeters (DSC) Thermogravimetric Analyzers (TGA) High Pressure Thermogravimetric Analyzers (HP-TGA) Simultaneous Thermal Analyzers (SDT) Dynamic Mechanical Analyzers (DMA) Thermomechanical Analyzers (TMA) Sorption Analyzers (SA) Dilatometers Horizontal Dilatometers 7 0 obj A new self-aligning mechanism ensures the parallelism of upper and lower plates, enhancing strain and force uniformity while simplifying user interaction and improving modulus accuracy and precision. Price: Please Inquire. TA Instruments. ElectroforceTesting Solutions for DMAWhats New in WinTest 8.0 Release Notes. You can go from melt rheology to solids testing with a simple geometry swap. Click the Advantage Software v5.5.24 link on this page to start the download. Tan can provide information on the overall flexibility and the interactions between the components of a composite material. It is the only motor in theindustry backed by a ten-year warranty. Note: This software supports TAM Air instruments. The software can be installed offline on any computer for easy sharing of data with colleagues. * Testing above 500C requires high temperature sample clamps. FB m!IqkPl ?;-E_ endobj TA Instruments pioneered DMA instrumentation with the 980 DMA introduced in 1976 and continues the tradition today. The DMA 3200 motor delivers a force output of up to 500 N and controlled displacements ranging from 1 micron to 13 mm. The superior measurement sensitivity of the HR 30 and flat baseline of the Discovery DSC deliver measurement quality you can depend on. TA Instruments ElectroForce DMA 3200 High Force DMA. The sample chamber accommodatesstandard DMA clamps (tension, cantilever, and 3-point bending). endobj Insights into polymer characteristics and processing conditions are only as accurate as the measurements themselves. The wide range of TA Dynamic Mechanical Analyzers is not only the best-selling in the world, but also covers the widest range of forces and applications. Its measurements extend beyond simply quantifying the magnitude of force divided by the displacement magnitude; it accurately calculates the phase relationship between the signals. G> O&/#pW82_={y_sR;A.iJrQ0JM6)u1TEt2W|j}jp'b5'^GXHc~^4\Xro1\mhKchH+ozaP&c?-%XZB("WE1]RcvXI',I/ =]9*vE9|* Q0dTiMvKZi ~VnxA!|^&Wc?9Jrjp`! Standard Furnace The Standard Furnace for the DMA 850 is a wide-range bifilar wound furnace that provides. Automated custom report generation including: experimental details, data plots and tables, control charts and analysis results. The standard compression kit includes parallel plates of 15 mm and 40 mm diameter, ideally designed for bulk measurements of moderate to low stiffness samples. Materials such as polymers exhibit viscoelastic behavior which is directly related to molecular structure and formulation differences. Discover powerful TRIOS software that delivers exceptional user experience in a combined package for instrument control, data analysis and reporting. water or solvents), semi-solid or soft gels, to high stiffness and high modulus solids. A newly designed film tension clamp simplifies the clamping mechanism to improve ease-of-use, clamping uniformity, and effectively prevents sample slippage. TA Instruments Testing can be conducted in both static and dynamic modes. DMA testing is driven by TAs patented transducer technology, so no extra hardware is needed. The ARES-G2 is the most advanced rotational rheometer for research and material development. Introduction Compression Clamp Installation & Calibration for the DMA 850 TATechTips 3.54K subscribers Subscribe 7 Share 3.3K views 4 years ago Rheology Check out our website or subscribe to our. Axial Force Control moves the cross-head such that the clamp maintains continuous contact with the sample. Viscoelastic measurements can be used to gain insight into the molecular weight and molecular weight distribution, while DSC can be used to examine the impact of thermal history and formulation changes on the polymer properties and crystallization behavior. This field-proven design provides for efficient and precise temperature control over the entire temperature range in heating, cooling, and isothermal operation. The DMA 3200 features patented ElectroForce linear motor technology enabling a single instrument to deliver unequalled performance and data accuracy. The Scarabaeus Software system for instrument control and analysis integrates and organizes data from multiple instruments and historical tests. Features such as automated calibration routines and real-time test method editing provide unmatched flexibility, while One-Click analysis and custom reporting raise productivity to new levels. Thermal Conductivity & Diffusivity Analyzers, High Pressure Thermogravimetric Analyzers (HP-TGA), Discovery Hybrid Rheometer (DHR) Accessories, Nano Differential Scanning Calorimeter (DSC), ElectroForce Mechanical Testing Accessories, Thermal Conductivity & Diffusivity Brochures, ElectroForce Mechanical Testing Brochures, High Force DMA & Fatigue Test Instruments, Dielectric Thermal Analysis Accessory (DETA), Single and Dual Cantilever (Clamped Bending), Axial Force Control tracks material stiffness and automatically adapts static load, AutoStrain adjusts applied strain to changing sample stiffness, Responsive FCO temperature control: -150 C to 600 C. The patented, frictionless Electroforce motortechnology, superior mechanical design, efficientenvironmental control, and wide variety of clampingsystems deliver superior data accuracy for the broadestrange of applications. The tension clamp is fortensile testing of thin films, strips, bars and individualfibers and fiber bundles. The ultra-stiff design of the 3200 ensures superior data accuracy. Standard FCO clamps, constructed of 17-4 stainless steel, are for use to a maximumtemperature of 500C, with optional clamps available for extended use to 600C. Users who have yet trained are not permitted to operate any lab instruments. . The FCO comes standard with a convenient long-life internal LED light and viewing port. In addition, the frictionless, moving-magnet design eliminatesfailure points that exist in other motor designs, such as movingwires and bearing degradation. The DMA measurements were performed on a DMA 2980 Dynamic Mechanical Analyser (TA Instruments, Inc.) in two different modes, the DMA "multi-strain" (MS-mode) and "controlled force" (CF-mode) mode. This enables a DMA instrument to quantify the elastic (spring-like) versus viscous (fluid-like) components of the sample response which is crucial for reliable and complete viscoelastic property characterization such as Storage Modulus, Loss Modulus, and Tan delta. Discovery DMA 850 - The Most Powerful Dynamic Mechanical Analysis With this data, you will save time and money by optimizing processing conditions such as extrusion operating temperatures, extrusion speed, blow molding and injection molding times, die swell, and more. Tracking the cure reaction in real-time with the HR 30s low torque performance, allows you to clearly pinpoint the minimum viscosity and gel point with confidence. TAM IV & IV-48. %PDF-1.5 Advance your polymer lab by combining multiple techniques, Differential Scanning Calorimeter (DSC 2500), Application Note Assessing the Effects of Process Temperature on Crystallization Kinetics of Polyphenylene Sulfide Utilizing Differential Scanning Calorimetry (DSC), Effect of Thermal Degradation on Polymer Thermal Properties, Identification of a Cross-Linked Rubber by Evolved Gas Analysis and Thermal Analysis Techniques, Assessing the Effects of Process Temperature on Crystallization Kinetics of Polyphenylene Sulfide utilizing DSC, Comparison of Crystallization Behavior of Different Colored Parts Made from Polypropylene using a Single DSC Experiment, Connecting Polymer Processing and Product Performance through Rheology and DMA, Thermal, Rheological, and Mechanical Characterization of Thermosets, Characterizing Polymer Properties for Compound Formulation: Determining Polymers that Lead to Successful Products, Strategies for Rheological Evaluation of Adhesives, Characterization of Active Shape-Memory Polymers, Extensional Rheology in Polymer Processing, The Role of Interfacial Elasticity on the Rheological Behavior of Polymer Blends, Patented, linear motor and high-resolution displacement sensor provides unmatched control over the widest ranges of force, displacement, and frequency, for superior data accuracy, Ultra-durable, frictionless motor, backed by industrys only ten-year warranty, provides maintenance- and worry-free operation, High force of 500 N enables testing of larger samples or final parts under real-world conditions, by achieving higher loading levels in both DMA and fatigue analysis, Forced Convection Oven (FCO) provides superior control and responsiveness over a temperature range of -150C to 600C for the highest degree of accuracy and flexibility in experiment thermal profiles, Large Sample Oven (LSO), with a temperature range of -150C to 315C, offers spacious interior dimensions to accommodate testing of large samples or components, Air Chiller Systems (ACS) offer unique gas flow cooling for sub-ambient testing without the use of liquid nitrogen, eliminating potential laboratory hazards while providing an incredible return on investment, Broad range of fixtures accommodate a wide range of sample sizes and geometries adding to testing versatility, Extremely rigid test frame and air bearings ensure the most accurate results on samples of very high stiffness, Multi-color status lights provide clear and visible indication of instrument and test status, WinTest and TRIOS Software packages provide powerful and easy-to-use instrument control and data analysis for the ultimate flexibility in experimental design, TRIOS Software providing extreme testing flexibility, Large Amplitude Oscillatory Shear (LAOS) and Fourier Transform (FT) Rheology, NEW Orthogonal Superposition (OSP) and 2 Dimensional Small Amplitude Oscillatory, NEW DMA mode for measurements of solids in bending, tension and compression. The high-force capability of the DMA 3200 extends experimental loading regimes and enables testing of larger samples or actual components. A rotational rheometer can perform flow measurements to test the viscosity of a liquid as a function of time, temperature shear rate or shear stress. Price: Please Inquire. Alternatively the FCO can be cooled to as low as -100C using LN2 free Air Chilling Systems. The DMA Mode adds a new dimension for testing of solid and soft-solid materials. TA Instruments 3.1K views3 years ago Discovery DMA 850 - The Most Powerful Dynamic Mechanical Analysis TA Instruments 11K views5 years ago Rheology Play all Auto-Trim Accessory for the. Overall this approach helps to get an idea how big the CTE is but more. Thermal Analysis 2 Rheology - DHR & AR 9 Rheology - ARES-G2 & ARES Classic 25 Rubber Testing 32 RSA-G2 33 DMA Q800 34 Microcalorimetry - TAM Systems 36 Microcalorimetry - Nano Systems 41 Thermophysical Properties 43 TA Instruments Registered Trademarks Mechanical fatigue testing provides insights on how and when materials, components, or devices fail when subjected to oscillating forces, or stresses. Prediction of impact resistance, testing of creep or cold flow, cure behavior. <> Properties measured by TA Instruments DSC techniques include glass transitions, cold crystallization, phase changes, melting, crystallization, product stability, cure / cure kinetics, and oxidative stability. Two equal-size pieces of the same material are sheared between a fixed and moving plate for the measurement of shear modulus, G. This mode is ideal for soft materials such as gels, pressure sensitive adhesives, and high viscosity resins. The new linear autosampler was designed to be even more rugged and simpler to use than ever before. True axial DMA capability in bending, tension, and compression. In this design, air is passed over tworesistive elements and into the cavity, optimizing uniformity over large volume for temperature control from -150C to 315C. Minimizing instrument component deformations, or compliance, reduces displacement measurements that can otherwise appear to be sample deformation. April 27, 2023 - TA Instruments Thermal Analysis Instruments | New and Used DSC, TGA - LabX Microcalorimetry Brochures. Repair and maintenance will be done on best-effort after 2024. This efficient, quiet, and lubrication-free motor technologyallows the DMA 3200 to be used virtually anywhere; from labto production floor, or from the cleanroom to office space. High Force DMA & Fatigue Test Instruments. The DMA 850 offers your choice of two dedicated environmental systems: the Standard Furnaceand the DMA-RH Accessory for humidity and temperature control. 3-point bending, or free bending, is often considered a pure mode of deformation because clamping effects are eliminated. If you do not have an Orchestrator security key please call your TA Instruments Technical Sales Representative for assistance. TA Instruments Dynamic Mechanical Analyzer (DMA) Q800 provides state-of-the-art and high precision measurement of solid and bulk materials versus temperature, time, and frequency. TA Instruments. endobj The sample demonstrates the classic linear region in the beginning of the test in the left of the plot and a very long ductile failure over the middle and right of the plot. 5 0 obj This test demonstrates how the DMA 3200 can be used for a high cycle test, leveraging its high acceleration and durability attributes. Process optimization oven temperature, molding times, and more. Common usage includes investigation, selection, comparison and end-use performance evaluation of materials in research, quality control and production applications. Lifetime Predictions Using Time Temperature Super Positioning, Location: Thermal Analysis, Rheology, and Polymer Processing Lab This efficient, quiet, and lubrication-free motor technology allows the DMA 3200 to be used virtually anywhere; from lab to production floor, or from the cleanroom to office space. These features work in concert to ensure the highest quality data on all samples and conditions with minimal experimental optimization. Dynamic mechanical analysis (DMA) is the most preferred widely used and thermal analysis technique for determining the glass transition temperature ( Tg ) of polymer matrix composites because it is more sensitive to Tg measurements than other thermal analysis techniques. This download is a full version of the software and documentation. PDF William J. Hughes Technical Center Atlantic City International Airport This powerful oven can heat at rates up to 60C/min. All rights reserved. The DMA 3200 features aHigh Accuracy Displacement Sensor (HADS),for the purest control and measurement of the small and large deformations necessary for DMA and fatigue testing. Collect the appropriate amount of data for your test by selecting one of four data acquisition modes Configurable and reliable for tests ranging in duration from 10 milliseconds to 10 months.